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Beilstein J. Org. Chem. 2017, 13, 2883–2887, doi:10.3762/bjoc.13.280
Graphical Abstract
Scheme 1: The synthesis of anti-2,3-difluorobutan-1,4-diol (anti-5) [17].
Scheme 2: Improved epoxide opening and deoxofluorination conditions.
Scheme 3: Attempted synthesis of anti-5 via acetonide protection.
Scheme 4: Completion of the synthesis of anti-5.
Scheme 5: Synthesis of (±)-syn-5.